| Crystal data |
| Chemical formula |
[Rh(NO)(NO2)2(C18H15P)2] |
|
M
r
|
749.48 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
10.2732 (2), 10.3317 (2), 18.1514 (4) |
| α, β, γ (°) |
90.118 (2), 105.089 (2), 118.323 (2) |
|
V (Å3) |
1619.50 (6) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
5.60 |
| Crystal size (mm) |
0.17 × 0.1 × 0.03 |
| |
| Data collection |
| Diffractometer |
Rigaku XtaLAB Synergy-S |
| Absorption correction |
Multi-scan (SCALE3 ABSPACK; Oxford Diffraction, 2005 ▸) |
|
Tmin, Tmax
|
0.850, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
38997, 6535, 6126 |
|
R
int
|
0.047 |
| (sin θ/λ)max (Å−1) |
0.625 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.030, 0.082, 1.08 |
| No. of reflections |
6535 |
| No. of parameters |
487 |
| No. of restraints |
160 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.50, −1.04 |
