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. 2025 Jul 24;14(15):2284. doi: 10.3390/plants14152284

Table 3.

Examples of plant waste extracted with conventional and non-conventional methods and analysed by liquid chromatography-mass spectrometry with the identification of different classes of compounds.

Plant Waste Extraction Methods Analytical Techniques Bioactive
Compounds
Ref.
Wine lees Maceration followed by microfiltration step UHPLC-LTQ Orbitrap and Velos LC-QTrap 4000 Phenolic compounds [91]
Olive leaves Organo-solv extraction LC-Finnigan AQA Polyphenols [92]
Tomato pomace Maceration LC-Q-Exactive Polyphenols [93]
Spent black tea Pressurised liquid extraction LC-LTQ-Orbitrap XL Phenolic compounds [94]
Aloe vera leaf UAE and MAE extractions LC/MS single quadrupole Anthraquinone and chromone derivatives [95]
Olive mill wastewater Liquid-liquid extraction LC-QTRAP 6500 Polyphenols [58]
Saffron tepals Enzymatic and subcritical water extractions LC-LTQ XL linear ion trap Flavonoids [96]
Red cabbage waste Pressurized liquid extraction (PLE), ultrasound-assisted extraction (UAE), and heating and stirring extraction (HSE) LC-Linear Ion Trap Anthocyanyns [99]
Annatto by-product Maceration UPLC-MS/QTOF Analysis Terpenoids, ceramides [41]
flower P. serrulata Maceration LC-Q-Trap 6500 in MRM mode Anthocyanins [64]
Plum seed residue Matrix solid-phase dispersion HPLC-ESI-QTOF-MS Phenolic compounds [37]
Walnut husk and pellicle Ultrasound UHPLC-Q-Exactive Flavonoids, tannins and quinones [38]
Chia leaves Maceration UHPLC-Q-Exactive Polyphenols [39]
Peach by-product Extraction with enzyme (EAE) UPLC-Qexactive Phenolic acid
Flavonoids
[40]
Mustard, kale, and broccoli microgreens Maceration UHPL-Fusion Orbitrap Flavonoids [43]
Foxnut Maceration LC-Orbitrap eclipse Lipids, amino acids, phenolic acid
Flavonoids alkaloids
[44]
Roots of red beet and sugar beet Maceration LC-LTQ XL linear ion trap Betalins
Phenolic compounds
[59]
Peel of Citrus retigulata Ultrasound extraction LC-Q-Exactive Flavonoids [63]
Fennel waste Ultrasound extraction UPLC-Qtrap 6500 Flavonoids [66]
Apple cider by-products Maceration LC-Q-TOF Carotenoids, phenols [85]
Tamarillos Maceration LC-APCI-MS/MS Carotenoids [100]
Red pepper skin Maceration LC-Q-Exactive Carotenoids [102]
Avocado Maceration UHPLC-Q-Tof Phenolic acids [108]
Mango peel Maceration LC-ESI-MS Polyphenols [109]