Table 3.
TAK-981 benchtop stability in human K2EDTA plasma.
| Run Number | LQC 0.300 ng/mL | HQC 75.0 ng/mL | Dil 20 QC 1,000 ng/mL |
|---|---|---|---|
| 3 | 0.319 | 73.4 | 1,060 |
| Stored at 4°C | 0.315 | 75.9 | 1,070 |
| for 24 hours | 0.316 | 75.2 | 990 |
| 0.346* | 78.2 | 1,060 | |
| Mean | 0.324 | 75.7 | 1,050 |
| S.D. | 0.0148 | 1.99 | 37.0 |
| %CV | 4.6 | 2.6 | 3.5 |
| %RE | 8.0 | 0.9 | 5.0 |
| n | 4 | 4 | 4 |
Note: *: Deviation from nominal > 15%; value included in statistics.
%CV: percent coefficient of variation; %RE: percent relative error; Dil 20 QC: 20-fold dilution QC; HQC: high-quality control; LQC: low-quality control; n: number; S.D.: standard deviation.