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. 2025 Feb 26;263(7):1765–1787. doi: 10.1007/s00417-025-06773-1

Table 2.

Summary of controlled trials evaluating the use of reduced eyedrop volume compared with standard drops

Author, year Design Population
(sample size)
Regimen(s) Instilled drop volumes (level of comparison, i.e., eyes or subjects) Method of instilling microdrops Efficacy outcome(s) Safety outcome(s)
a1-adrenergic agonists and muscarinic antagonists
Brown 1978 [11] Non-randomized controlled trial

Adults

(41)

Group A

- µ-drop of PHE 5% & TRO 0.5%, in a mixture, in one eye

(1 drop, 3 doses, 5 min interval)

- s-drop of PHE 10% & TRO 1%, sequentially, in the other eye

(1 drop, 3 doses, 5 min interval)

Group B

- µ-drop of PHE 5% & TRO 0.5%, in a mixture, in one eye

(1 drop, 3 doses, 5 min interval)

- s-drop of PHE 10% & TRO 1% in the other eye

(1 drop, 3 doses, 5 min interval)

A) 5 µl vs. 70 µl

(in either eye of the same subject)

B) 10 µl vs. 70 µl

(in either eye of the same subject)

A) Sterile PE-160 polyethylene tubing wrapped at least four times around the barrel of a 1-ml tuberculin plastic syringe and attached to the syringe through an 18-gauge needle

B) Calibrated micropipette

A) Mean pupil diameter at T45 increased from 2.09 mm to 7.10 mm after µ-drop, and from 2.10 mm to 7.39 mm after s-drop

B) No difference in mydriasis between µ-drop and s-drop

Tearing and ocular irritation experienced only after s-drop (percentages are not reported)
Brown 1987 [130] Crossover RCT

Adults

(10)

- µ-drop of PHE 10%

(1 drop, 2 doses, 10 min interval)

- s-drop of PHE 2.5%

(1 drop, 2 doses, 10 min interval)

8 µl vs. 32 µl

(subjects, at least one-week washout period)

Calibrated micropipette Larger increase from baseline in pupil diameter at T45 after µ-drop (p = 0.0001) No difference in the average plasma concentration of PHE at T10, T20, T40
Lynch 1987 [13] RCT

Preterm infants

(11 for efficacy and 17 for safety outcome)

PHE 2.5%

(1 drop, 3 doses, 2–5 min interval)

8 µl vs. 30 µl

(eyes for the efficacy and subjects for the safety outcome)

Calibrated micropipette No difference in the percent change from baseline in pupil diameter at T60 Lower plasma levels of PHE at T10 after µ-drop (p = 0.01)
Craig 1991 [131] Crossover non-randomized controlled trial

Healthy volunteers

(20)

PHE 10%

(regimen NR)

10 ± 2 µl vs. 30 ± 4 µl

(subjects, one week washout period)

22G Venflon iv cannula attached to the end of a Minim after removal of the central stylette No difference in the change from baseline in pupil diameter at T60 Less discomfort was self-reported after µ-drop (percentages are not reported)
Gray 1991 [132] RCT

Patients requiring diagnostic pupil dilation

(60)

Group A: PHE 10% & TRO 1%

(1 drop of each, 2 min apart)

Group B: TRO 1%

(1 drop)

Group C: TRO 0.5%

(1 drop)

5 µl vs. 26 µl

(in either eye of each subject in all three groups)

30G Rycroft cannula attached to the minim

A) Larger increase in pupil diameter at T20 after s-drop

B) No difference in the change from baseline in pupil diameter at T20

C) Larger increase in pupil diameter at T20 after s-drop

Less ocular discomfort was reported after µ-drop (percentages are not reported)
Gray 1992 [133] Crossover non-randomized controlled trial

Healthy adult volunteers

(20)

TRO 1%

(Regimen NR)

5 µl vs. 26 µl

(subjects; only one eye was tested in each individual, at least one-week washout period)

Narrow bore cannula attached to the minim No difference in the change in pupil: cornea diameter ratio at T30, T60, T120 and T240 Improved rate of recovery of distance and near visual acuity at T30 after µ-drops compared with s-drops (p < 0.05)
Noske 1993 [14] Crossover non-randomized controlled trial

Children with uncorrected or undercorrected hypermetropia

(15)

Atropine 0.5% (< 2 years)

− 1 µ-drop, 3 doses, 5 min interval

− 1 s-drop, 6 doses (twice daily for 3 days)

Atropine 1% (> 2 years)

− 1 µ-drop, 3 doses, 5 min interval

− 1 s-drop, 6 doses (twice daily for 3 days)

5 µl vs. 30–36 µl

(eyes, without washout period)

Calibrated micropipette

Higher by 0.25 D mean spherical equivalent of cycloplegic refraction at T90 after s-drop (p < 0.05)

No difference in cylindrical power and axis after s-drop and µ-drop

Increased change from baseline in HR at T90 after s-drop (p < 0.05)

Typical flushing observed in some children after both

s-drop and µ-drop

Wheatcroft 1993 [134] Non-randomized controlled trial

Preterm infants

(26)

PHE 2.5% & CYCLO 0.5%

(1 drop of each, 5 min apart)

5 µl vs. 26 µl

(in either eye of the same subject)

30-gauge Rycroft intraocular cannula attached to the minim No difference in pupil diameter at T40-T60 Not assessed
Whitson 1993 [12] Crossover RCT

Healthy adults

(13)

PHE 10%

(1 drop, 2 doses, 10 min interval)

+/- eyelid closure for 1 min

10 µl vs. 30 µl

(subjects, at least one-week washout period)

Calibrated micropipette

No difference in pupil diameter at T60

For both s-drop and µ-drop, eyelid closure produced greater pupil dilation

No difference in plasma concentration at T20
Elibol 1997 [135] Crossover non-randomized controlled trial

Infants

(53)

Group A: PHE 10%

(1 drop, 2 doses, 5 min interval)

Group B: CYCLO 1%

(1 drop, 2 doses, 5 min interval)

Group C: TRO 0.5%

(1 drop, 2 doses, 5 min interval)

A) 5.1 µl vs. 33 µl

(subjects, 3–7 days washout period)

B) 6.5 µl vs. 39.2 µl

(subjects, 3–7 days washout period)

C) 5.4 µl vs. 33.8 µl

(subjects, 3–7 days washout period)

24-gauge intravenous cannula attached to the end of a minim after removal of the central stylette

A) No difference in pupil diameter at T15, T30, T45, T60

B) No difference in pupil diameter at T15, T30, T45, T60

C) Increased pupil diameter at T30, T45, T60 after s-drops compared with µ-drops (p < 0.01)

A, B, C) Increased change from baseline in mean BP at T15, T30, T45, T60 after s-drop (p < 0.01)

A, B, C) No difference in the change from baseline in HR at T60

B, C) Significant flushing after s-drop of CYCLO and TRO compared with µ-drop (p < 0.01)

Ianchulev 2016 [136] RCT

Healthy adults

(102)

PHE 2.5% & TRO 1%, sequentially

Group A: 1 µ-drop * 1.5 µl of each drug in one eye

Group B: 2 µ-drops * 3 µl of each drug in one eye (3-min interval)

Group C: 1 µ-drop * 6 µl of each drug in one eye

In all three groups: 1 s-drop (26 µl) of each drug in the other eye

1.5–3 µl or 6 µl vs. 26 µl

(in either eye of the same subject)

Piezoelectric device No difference in pupil diameter at T10, T20, T60 min after instillation of 2*3 µl and 1*6 µl compared with s-drops Participants preferred piezoelectric self-delivery to s-drops, reporting better head-positioning comfort, reduced tearing/overflow and increased likelihood of adhering to ocular medication regimens (p < 0.0001)
Ianchulev 2018 [137] Crossover non-randomized controlled trial

Healthy adults

(12)

Group A: s-drop of PHE 10%

(Regimen NR)

Group B: s-drop of PHE 2.5%

(Regimen NR)

Group C: µ-drop of PHE 10%

(Regimen NR)

8 µl vs. 32 µl

(subjects, one-week washout period)

Microdroplet spray device

No difference in the change from baseline in pupil diameter at T30, T45, T60

µ-drop of PHE 10% achieved comparable pupil dilation as s-drop of PHE 10%, and superior pupil dilation to s-drop of PHE 2.5% at T75 (p = 0.009)

No difference in HR and BP at T60

No difference in PHE plasma levels at T20 after µ-drop of PHE 10% or s-drop of PHE 10%

Higher PHE plasma levels at T20 after µ-drop of PHE 10% compared with s-drop of PHE 2.5% (p = 0.021)

Seliniotaki 2022 [125] Pilot crossover RCT

Preterm infants

(25)

PHE 1.67% & TRO 0.33% (mixture)

(1 drop, 3 doses, 5 min interval)

6–7 µl vs. 28–34 µl

(subjects, one-week washout period)

27-gauge irrigating cannula attached to a disposable 2.5 ml syringe No difference in pupil diameter at T45, T90, T120

No difference in HR at T45, T90

Lower levels of HR at T120 after µ-drop (p = 0.046)

No difference in BP and oxygen saturation at T45, T90, T120

No difference in 24-h cardiorespiratory and gastrointestinal AE

Hoppe 2023 [138] Non-inferiority RCT

Children

(50)

PHE 2.5% & CYCLO 1% & TRO 1%

(1 drop of each drug sequentially)

10.4 µl vs. 50 µl

(eyes)

Nanodropper adaptor

Inconclusive trial regarding spherical equivalent and pupil constriction percentage** at T30

Non-inferiority of µ-drop compared with s-drop regarding pupil diameter at T30 (non-inferiority margin: −0.20)

Inconclusive trial regarding IOP after dilation
Seliniotaki 2024 [139] Non-inferiority crossover RCT

Preterm infants

(83)

PHE 1.67% & TRO 0.33% (mixture)

(1 drop, 3 doses, 5 min interval)

6.5 µl vs. 28–34 µl

(subjects, at least one-week washout period)

Calibrated micropipette

Superiority of µ-drop regarding pupil dilation at T45 (p = 0.008)

Non-inferiority of µ-drop regarding pupil dilation at T90 and T120 (Bonferroni-corrected 95%CI at T90: −0.10, 0.17; at T120: −0.18, 0.14; non-inferiority margin: −0.4 mm)

Lower levels of oxygen saturation at T45 (p = 0.03) and T90 (p = 0.04) after s-drop

Higher percentage of 24 h hypertensive episodes (p = 0.01) after s-drop

Pooled pharmacokinetic data of PHE within 3-hours post-instillation, insufficient to compare µ-drop with s-drop

beta-blockers
Montoro 1990 [94] RCT

Adults

(20)

Timolol maleate 0.5%

(Regimen NR)

29.12 ± 1.2 µl vs. 49.26 ± 1.4 µl

(subjects; before-after)

NR

Significant reduction in IOP in each separate group

(time-point not specified)

Decrease in HR from baseline in each separate group – larger decrease observed after s-drop (0.05 < p < 0.10)

No difference in BP compared with baseline in each separate group

Steger 2024 [98] Non-inferiority RCT

Adults with open angle glaucoma and ocular hypertension

(419)

Timolol maleate 0.5%

(1 drop)

12.5 µl vs. 28 µl

(subjects)

Nanodropper adaptor

Significant reduction in IOP in each separate group at all time-points (1-, 2-, 5- and 8-hours post-instillation)

Non-inferiority of µ-drop regarding IOP at 1-, 2-, and 8-hours post-instillation (non-inferiority margin: 1.5 mmHg)

Inconclusive trial at 5-hours post-instillation

Significant reduction in systolic BP in each separate group at 1-, 2-, and 5- hours post-instillation)

No difference in diastolic BP change from baseline in each group at any time-point

Greater absolute and relative HR decrease from baseline after s-drop

a2-adrenergic agonists
Petursson 1984 [15] Crossover RCT

Adults

(16)

Placebo in one eye &

Clonidine 0.25% or Clonidine 0.5%

in the other eye

(1 drop)

15 µl vs. 70 µl

(eyes)

Calibrated pipette Both s-drop and µ-drop of 0.25% and 0.50% clonidine lowered the IOP at 1–5 h compared with the placebo

Only s-drop of 0.50% clonidine lowered systemic BP at 1–5 h

Transient “burning in the eye” after µ-drop of clonidine 0.25% (one patient)

Vocci 1992 [140] Crossover RCT

Healthy adult volunteers

(29)

Apraclonidine 0.5%

(1 drop)

16 µl vs. 30 µl

(subjects, one-week washout period)

A potentially commercially available eyedrop bottle that delivers 16 µl

No difference in mean IOP at 1, 3, 8, 12 h

Reduced IOP at 1, 3, 8, 12 h after s-drop and µ-drop compared with placebo

No difference in the % change from baseline in BP

No difference in the number of subjects experiencing AE including blurred vision, dry mouth, drowsiness, tiredness

muscarinic agonists
File 1980 [16] Crossover RCT

Healthy adult volunteers

(10)

Pilocarpine 0.5%

(1 drop)

20 µl vs. 50 µl

(subjects; only one eye was tested in each individual, one-week washout period)

Micropipette with sterile disposable tips No difference in the change from baseline in pupil diameter up to 2 h post-instillation Not formally assessed
Lal 1995 [141] Crossover RCT

Healthy volunteers

(12)

Pilocarpine 2%

(1 drop)

after the drop administration, the inner punctum was pressed for 1 min

10 µl vs. 20 µl vs. 40 µl vs. 80 µl

(subjects, 7-days washout period)

Micropipette Larger decrease in pupil diameter at T15, T30, T45, T60, T90, T120, T180, T240, T300 after 10 µl, compared with 20 µl, 40 µl and 80 µl

No difference in HR at T15, T30, T45, T60, T90, T120, T180, T240, T300

Fewer subjects experiencing frontal headache or ocular irritation after 10–20 µl (statistical analysis not performed)

allogeneic serum
Vermeulen 2023 [142] Multi-center non-inferiority crossover RCT

Adults with dry eye disease

(49)

Allogeneic serum

(6 drops daily for 1 month)

7 µl vs. 50 µl

(hospitals, one-month washout period)

mu-Drop system Non-inferiority of µ-drop compared with s-drop regarding the Ocular Surface Disease Index score (mean difference − 2.60; 95%CI −9.16 to 3.97; p = 0.006; non-inferiority margin = 6) Not formally assessed

µ-drop microdrop instillation, s-drop standard drop instillation, PHE phenylephrine, TRO tropicamide, CYCLO cyclopentolate, RCT randomized controlled trial, BP blood pressure, HR heart rate, NR not reported, IOP intraocular pressure, AE adverse events, ROP retinopathy of prematurity, CI confidence interval 

**Pupillary constriction percentage was calculated by the pupillometer in response to a 180-mW flash: (maximum - minimum) / maximum