Table 12. Comparison of SMA's catalytic efficiency for the synthesis of 4a with that of other catalytic systems.
| Catalyst | Amount of catalyst | Yield (%) | Solvent | Time (min) | Temperature (°C) |
|---|---|---|---|---|---|
| SmCl3 (ref. 57) | 20 mol% | 98 | — | 540 | 120 |
| CAN59 | 5 mol% | 96 | PEG 400 | 240 | 50 |
| SbCl3/SiO2 (ref. 60) | 10 mol% | 93 | — | 50 | 120 |
| Sr(OTf)2 (ref. 61) | 10 mol% | 85 | DCM | 300 | 80 |
| H14[NaP5W30O110]62 | 0.4 mol% | 88 | — | 120 | 120 |
| SMA (this work) | 1 mol% | 98 | IPA | 80 | 70 |