| Crystal data |
| Chemical formula |
(C6H14NO2)2[SnCl6]·2H2O |
|
M
r
|
631.78 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
10.9838 (11), 10.7837 (11), 10.8556 (11) |
| β (°) |
102.316 (4) |
|
V (Å3) |
1256.2 (2) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.68 |
| Crystal size (mm) |
0.17 × 0.13 × 0.11 |
| |
| Data collection |
| Diffractometer |
D8 VENTURE Bruker AXS |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.769, 0.831 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
13707, 5560, 5406 |
|
R
int
|
0.024 |
| (sin θ/λ)max (Å−1) |
0.649 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.021, 0.052, 1.08 |
| No. of reflections |
5560 |
| No. of parameters |
255 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.14, −0.96 |
| Absolute structure |
Flack x determined using 2423 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
−0.004 (10) |
