Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Sn(C6H5)2I(OH)]·2C6H12N2O |
| M r | 1089.95 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 10.1014 (4), 11.3064 (4), 17.1982 (7) |
| β (°) | 93.027 (2) |
| V (Å3) | 1961.47 (13) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.89 |
| Crystal size (mm) | 0.30 × 0.18 × 0.09 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.482, 0.671 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 100676, 4729, 4323 |
| R int | 0.079 |
| (sin θ/λ)max (Å−1) | 0.661 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.024, 0.061, 1.05 |
| No. of reflections | 4729 |
| No. of parameters | 225 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.25, −1.47 |