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. 2025 Aug 21;10(Pt 8):x250711. doi: 10.1107/S2414314625007114

Table 2. Experimental details.

Crystal data
Chemical formula [Sn(C6H5)2I(OH)]·2C6H12N2O
M r 1089.95
Crystal system, space group Monoclinic, P21/n
Temperature (K) 100
a, b, c (Å) 10.1014 (4), 11.3064 (4), 17.1982 (7)
β (°) 93.027 (2)
V3) 1961.47 (13)
Z 2
Radiation type Mo Kα
μ (mm−1) 2.89
Crystal size (mm) 0.30 × 0.18 × 0.09
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Krause et al., 2015)
Tmin, Tmax 0.482, 0.671
No. of measured, independent and observed [I > 2σ(I)] reflections 100676, 4729, 4323
R int 0.079
(sin θ/λ)max−1) 0.661
 
Refinement
R[F2 > 2σ(F2)], wR(F2), S 0.024, 0.061, 1.05
No. of reflections 4729
No. of parameters 225
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 1.25, −1.47

Computer programs: APEX2 and SAINT (Bruker, 2009), SHELXS97 (Sheldrick 2008), SHELXL2014/7 (Sheldrick, 2015), DIAMOND (Brandenburg, 2006), Mercury (Macrae et al. (2020) and publCIF (Westrip, 2010).