Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C29H22F2N4O |
| M r | 480.50 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 8.4575 (4), 11.5163 (5), 23.0761 (10) |
| β (°) | 91.103 (2) |
| V (Å3) | 2247.17 (17) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.10 |
| Crystal size (mm) | 0.22 × 0.14 × 0.13 |
| Data collection | |
| Diffractometer | Bruker SMART APEXII area detector |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.688, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 15704, 5044, 3821 |
| R int | 0.030 |
| (sin θ/λ)max (Å−1) | 0.650 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.042, 0.113, 1.04 |
| No. of reflections | 5044 |
| No. of parameters | 325 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.30, −0.24 |