| Crystal data |
| Chemical formula |
C16H26NO+·Cl−
|
|
M
r
|
283.83 |
| Crystal system, space group |
Orthorhombic, Pna21
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
21.8109 (4), 8.2459 (2), 8.8751 (2) |
|
V (Å3) |
1596.19 (6) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
2.05 |
| Crystal size (mm) |
0.30 × 0.10 × 0.05 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE dual wavelength Mo/Cu |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.620, 0.754 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
22843, 3168, 3064 |
|
R
int
|
0.034 |
| (sin θ/λ)max (Å−1) |
0.625 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.029, 0.074, 1.06 |
| No. of reflections |
3168 |
| No. of parameters |
173 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.16, −0.21 |
| Absolute structure |
Flack x determined using 1329 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.014 (6) |
