TABLE 2.
Step | Vol (ml) | Total protein (mg) | Total activity (U) | Sp act (U/mg) | Fold | Recovery (%) |
---|---|---|---|---|---|---|
Crude enzyme | 500 | 1,500 | 3,300 | 2.2 | 1 | 100 |
(NH4)2SO4 precipitation | 400 | 600 | 2,460 | 4.4 | 2.0 | 80 |
Phenyl-TOYOPEARL 650M | 300 | 135 | 1,560 | 11.6 | 5.3 | 47 |
Q-Sepharose FF | 156 | 46 | 840 | 18.3 | 8.3 | 25 |
Enzyme activity was measured by using p-nitrophenyl acetate as a substrate.