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. 2025 Oct 7;13(41):17412–17421. doi: 10.1021/acssuschemeng.5c06980

1. Substrate Scope of the Amide Synthesis via an Extrusion-Based Leuckart-Type Approach .

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Experiments were run by reactive extrusion. Conditions: T = 150 °C; t = 15 min, screw rotation speed = 50 rpm; reactant aldehyde = 5 mmol; ammonium formate:aldehyde molar ratio = 3.