Table I. Data collection and refinement statistics.
Resolution (Å) | 2.1 |
Space group | P21212 |
Unit cell (Å) | 58.9, 59.5, 34.9 |
Molecules/asymmetric unit | 1 |
Rsym (% overall/2.16–2.1 Å shell) | 5.4/33.0 |
Reflections (total/unique) | 24 668/7460 |
Completeness (%) |
97.0 |
Refinement statistics | |
Resolution range (Å) | 20.0–2.15 |
Protein atoms | 908 |
Water molecules | 86 |
Rcryst/Rfree (%, F > 2σ) | 21.6/27.9 |
Rcryst (%, all data) | 23.1 |
R.m.s.d. bond length/angles | 0.016 Å/2.151° |