Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C29H31NO2 |
| M r | 425.55 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 300 |
| a, b, c (Å) | 13.2165 (8), 5.8983 (4), 31.503 (2) |
| β (°) | 99.174 (2) |
| V (Å3) | 2424.4 (3) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.07 |
| Crystal size (mm) | 0.36 × 0.22 × 0.16 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.975, 0.988 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 43823, 6019, 4053 |
| R int | 0.041 |
| (sin θ/λ)max (Å−1) | 0.667 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.052, 0.168, 1.03 |
| No. of reflections | 6019 |
| No. of parameters | 290 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.18, −0.20 |