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| Sr No | Parameter | Unit | Limit | Justification |
|---|---|---|---|---|
| 1 | Quantity of 16 | Equivalents | 4.0 | These are the minimum equiv required and studied during screening DoE |
| 2 | Quantity of 3 M HCl | Equivalents | 7.0 | |
| 3 | Volume of THF | Volume | 25 | No effect on responses, based on pre-DoE study |
