Table 2. Data collection and processing.
Values in parentheses are for the highest resolution shell.
| 14-3-3σ-ΔC–Sirt3pS103 | 14-3-3σ-ΔC–Sirt1pS670 | |
|---|---|---|
| PDB code | 8anc | 8anb |
| Diffraction source | BESSY BL14.1 | BESSY BL14.1 |
| Wavelength (Å) | 0.918409 | 0.918409 |
| Temperature (K) | 100 | 100 |
| Detector | PILATUS 6M | PILATUS 6M |
| Space group | C2221 | C2221 |
| a, b, c (Å) | 82.60, 112.38, 62.69 | 81.01, 95.55, 79.94 |
| Resolution range (Å) | 50–1.11 (1.18–1.11) | 50.0–1.64 (1.74–1.64) |
| Total No. of reflections | 390768 (50403) | 139781 (21387) |
| No. of unique reflections | 111534 (16525) | 38278 (6068) |
| Completeness (%) | 97.6 (90.2) | 99.6 (98.6) |
| 〈I/σ(I)〉 | 13.21 (2.16) | 18.32 (4.32) |
| CC1/2 | 99.9 (73.5) | 99.9 (91.0) |
| Rmeas (%) | 6.1 (62.7) | 5.0 (34.9) |
| Overall B factor from Wilson plot (Å2) | 12.916 | 26.983 |