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. 2026 Jan 1;82(Pt 1):91–95. doi: 10.1107/S2056989025011211

Table 3. Experimental details.

Crystal data
Chemical formula [Co(C8H5N2O2)2(C7H6N2)2]
M r 617.49
Crystal system, space group Monoclinic, P21/c
Temperature (K) 273
a, b, c (Å) 10.449 (4), 13.111 (5), 11.508 (5)
β (°) 113.427 (17)
V3) 1446.6 (11)
Z 2
Radiation type Mo Kα
μ (mm−1) 0.64
Crystal size (mm) 0.42 × 0.28 × 0.08
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Krause et al., 2015)
Tmin, Tmax 0.672, 0.754
No. of measured, independent and observed [I ≥ 2u(I)] reflections 3327, 3324, 1747
R int 0.050
(sin θ/λ)max−1) 0.651
 
Refinement
R[F2 > 2σ(F2)], wR(F2), S 0.119, 0.337, 1.01
No. of reflections 3324
No. of parameters 196
No. of restraints 120
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
Δρmax, Δρmin (e Å−3) 2.22, −1.92

Computer programs: APEX2 and SAINT (Bruker, 2014), OLEX2.refine (Bourhis et al., 2015), OLEX2 (Dolomanov et al., 2009), Mercury (Macrae et al., 2020), ShelXle (Hübschle et al., 2011) and PLATON (Spek, 2020).