Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Co(C8H5N2O2)2(C7H6N2)2] |
| M r | 617.49 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 273 |
| a, b, c (Å) | 10.449 (4), 13.111 (5), 11.508 (5) |
| β (°) | 113.427 (17) |
| V (Å3) | 1446.6 (11) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.64 |
| Crystal size (mm) | 0.42 × 0.28 × 0.08 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.672, 0.754 |
| No. of measured, independent and observed [I ≥ 2u(I)] reflections | 3327, 3324, 1747 |
| R int | 0.050 |
| (sin θ/λ)max (Å−1) | 0.651 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.119, 0.337, 1.01 |
| No. of reflections | 3324 |
| No. of parameters | 196 |
| No. of restraints | 120 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 2.22, −1.92 |