Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C16H13NO |
| M r | 235.27 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 4.89615 (14), 16.6590 (5), 14.2008 (4) |
| β (°) | 91.240 (3) |
| V (Å3) | 1158.02 (6) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.26 × 0.02 × 0.01 |
| Data collection | |
| Diffractometer | Rigaku XtaLAB P200K |
| Absorption correction | Multi-scan (CrysAlis PRO; Rigaku OD, 2024 ▸) |
| Tmin, Tmax | 0.714, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 24788, 2788, 1992 |
| R int | 0.055 |
| (sin θ/λ)max (Å−1) | 0.682 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.043, 0.124, 1.05 |
| No. of reflections | 2788 |
| No. of parameters | 164 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.30, −0.20 |