Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C22H24ClNO2 |
| M r | 369.87 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 298 |
| a, b, c (Å) | 8.7654 (5), 11.3919 (6), 11.6090 (7) |
| α, β, γ (°) | 110.594 (2), 102.709 (2), 107.595 (2) |
| V (Å3) | 962.71 (10) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.21 |
| Crystal size (mm) | 0.35 × 0.23 × 0.19 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.711, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 24328, 5355, 3183 |
| R int | 0.043 |
| (sin θ/λ)max (Å−1) | 0.706 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.050, 0.135, 1.03 |
| No. of reflections | 5355 |
| No. of parameters | 238 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.18, −0.27 |