Table 2. Experimental details.

Crystal data
Chemical formula	[U(C25H23O8)2O2(CH4O)]·C7H8
M r	1297.07
Crystal system, space group	Monoclinic, C2/c
Temperature (K)	170
a, b, c (Å)	15.392 (4), 23.149 (6), 15.907 (4)
β (°)	90.577 (9)
V (Å3)	5668 (3)
Z	4
Radiation type	Mo Kα
μ (mm−1)	2.94
Crystal size (mm)	0.25 × 0.18 × 0.12
Data collection
Diffractometer	Bruker APEXII CCD
Absorption correction	Multi-scan (SADABS; Krause et al., 2015 ▸)
Tmin, Tmax	0.595, 0.745
No. of measured, independent and observed [I > 2σ(I)] reflections	35282, 5389, 4061
R int	0.080
(sin θ/λ)max (Å−1)	0.613
Refinement
R[F2 > 2σ(F2)], wR(F2), S	0.054, 0.147, 1.12
No. of reflections	5389
No. of parameters	519
No. of restraints	561
H-atom treatment	H-atom parameters constrained
Δρmax, Δρmin (e Å−3)	1.50, −0.85

Computer programs: APEX2 and SAINT (Bruker, 2014 ▸), SHELXT (Sheldrick, 2015a ▸), SHELXL2018/3 (Sheldrick, 2015b ▸) and OLEX2 (Dolomanov et al., 2009 ▸).