Table 2.
13C NMR data of compounds 1–12 in CD3OD (δ in ppm, measured at 150 MHz)
| No | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 1 | 78.4 | 77.3 | 78.1 | 75.8 | 76.3 | 77.6 | 138.2 | 137.6 | 194.6 | 65.1 | 146.0 | 54.3 |
| 2 | 31.9 | 30.5 | 33.4 | 72.2 | 31.9 | 31.6 | 209.9 | 209.9 | 128.0 | 212.0 | 207.5 | 34.0 |
| 3 | 23.6 | 35.1 | 24.4 | 36.8 | 29.5 | 28.9 | 48.8 | 49.1 | 214.7 | 130.6 | 51.7 | 27.7 |
| 4 | 36.9 | 74.2 | 37.5 | 25.7 | 68.4 | 67.9 | 33.2 | 33.3 | 52.7 | 183.3 | 76.9 | 41.1 |
| 5 | 37.4 | 44.8 | 39.6 | 43.6 | 45.7 | 42.9 | 46.4 | 46.4 | 52.0 | 82.8 | 177.8 | 26.7 |
| 6 | 24.8 | 30.4 | 24.4 | 16.4 | 25.3 | 24.7 | 29.0 | 30.2 | 43.9 | 41.4 | 28.2 | 55.9 |
| 7 | 40.0 | 40.6 | 36.5 | 47.1 | 40.2 | 39.8 | 49.1 | 48.8 | 50.8 | 43.1 | 46.1 | 32.7 |
| 8 | 36.1 | 24.9 | 25.5 | 66.5 | 25.4 | 36.3 | 27.5 | 26.4 | 29.5 | 31.9 | 27.3 | 34.1 |
| 9 | 76.7 | 25.6 | 30.2 | 41.9 | 30.1 | 76.4 | 38.8 | 38.7 | 41.4 | 35.5 | 33.7 | 78.5 |
| 10 | 40.9 | 42.3 | 38.2 | 39.6 | 38.8 | 41.3 | 157.4 | 157.8 | 75.2 | 33.9 | 28.4 | 220.2 |
| 11 | 41.6 | 41.8 | 44.9 | 40.9 | 41.4 | 41.6 | 76.1 | 76.1 | 151.9 | 153.2 | 76.1 | 152.4 |
| 12 | 65.4 | 28.9 | 65.3 | 18.7 | 21.3 | 18.0 | 68.9 | 69.0 | 109.6 | 109.0 | 68.7 | 109.0 |
| 13 | 18.2 | 68.8 | 20.9 | 22.1 | 24.7 | 25.1 | 20.9 | 20.7 | 20.6 | 20.7 | 20.4 | 19.5 |
| 14 | 25.1 | 27.5 | 18.9 | 25.4 | 27.7 | 27.5 | 16.3 | 16.3 | 17.0 | 13.8 | 26.4 | 20.8 |
| 15 | 27.5 | 24.5 | 70.8 | 26.7 | – | – | 21.7 | 21.8 | 32.1 | 14.3 | 17.5 | 17.9 |