| Crystal data |
| Chemical formula |
C25H38N2O7S |
|
M
r
|
510.63 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
12.8909 (8), 7.5857 (4), 14.9027 (9) |
| β (°) |
103.924 (4) |
|
V (Å3) |
1414.46 (15) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
1.37 |
| Crystal size (mm) |
0.08 × 0.03 × 0.01 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE DUO PHOTON III |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.90, 0.99 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
16792, 4678, 3874 |
|
R
int
|
0.059 |
| (sin θ/λ)max (Å−1) |
0.597 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.044, 0.123, 1.02 |
| No. of reflections |
4678 |
| No. of parameters |
320 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.25, −0.23 |
| Absolute structure |
Flack x determined using 1374 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.034 (14) |
