Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C11H13NO2 |
| M r | 191.22 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 295 |
| a, b, c (Å) | 10.109 (1), 8.2598 (8), 12.2074 (13) |
| β (°) | 92.539 (4) |
| V (Å3) | 1018.30 (18) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.39 × 0.32 × 0.09 |
| Data collection | |
| Diffractometer | Bruker SMART X2S |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 12414, 2304, 1661 |
| R int | 0.037 |
| (sin θ/λ)max (Å−1) | 0.649 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.043, 0.131, 1.05 |
| No. of reflections | 2304 |
| No. of parameters | 135 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.16, −0.17 |