Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C10H11ClN2OS |
| M r | 242.72 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 293 |
| a, b, c (Å) | 11.971 (1), 4.1187 (6), 23.100 (2) |
| β (°) | 96.44 (1) |
| V (Å3) | 1131.8 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.50 |
| Crystal size (mm) | 0.50 × 0.48 × 0.36 |
| Data collection | |
| Diffractometer | Oxford Diffraction Xcalibur with Sapphire CCD detector |
| Absorption correction | Multi-scan (CrysAlis RED; Oxford Diffraction, 2006 ▸) |
| Tmin, Tmax | 0.790, 0.842 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 3971, 2291, 1809 |
| R int | 0.012 |
| (sin θ/λ)max (Å−1) | 0.625 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.043, 0.113, 1.10 |
| No. of reflections | 2291 |
| No. of parameters | 143 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.31, −0.25 |