Table 4.
Evaluation of precision study for determination of Marbofloxacin (MFC), Cefazolin (CFZ), and Sulfadimidine (SDD) by proposed HPTLC-densitometric method.
| Conc. (µg/band) | Intra-day (Repeatability) |
Inter-day (Intermediate precision) |
Pooled RSD (%) | |||||
|---|---|---|---|---|---|---|---|---|
| Mean conc. Found (µg/band) | Mean % recovery A ± SD | RSD (%) | Mean conc. Found (µg/band) | Mean % recovery A ± SD | RSD (%) | |||
| CFZ | 0.005 | 0.005 | 97.79 ± 0.458 | 0.469 | 0.005 | 98.11 ± 0.297 | 0.302 | 0.509 |
| 0.040 | 0.040 | 100.43 ± 0.482 | 0.481 | 0.040 | 99.79 ± 0.567 | 0.568 | ||
| 0.090 | 0.090 | 99.99 ± 0.434 | 0.434 | 0.091 | 101.06 ± 0.812 | 0.803 | ||
| MFC | 0.005 | 0.005 | 100.95 ± 0.523 | 0.518 | 0.005 | 100.87 ± 0.125 | 0.124 | 0.459 |
| 0.040 | 0.040 | 101.15 ± 0.679 | 0.671 | 0.040 | 100.63 ± 0.470 | 0.467 | ||
| 0.090 | 0.089 | 99.16 ± 0.811 | 0.818 | 0.089 | 99.00 ± 0.159 | 0.161 | ||
| SDD | 0.005 | 0.005 | 101.16 ± 0.083 | 0.082 | 0.005 | 100.65 ± 0.527 | 0.523 | 0.331 |
| 0.040 | 0.040 | 100.25 ± 0.354 | 0.353 | 0.040 | 100.33 ± 0.338 | 0.337 | ||
| 0.090 | 0.090 | 100.03 ± 0.407 | 0.407 | 0.090 | 100.33 ± 0.280 | 0.279 | ||
A Average of three determinations.