Table 1.
RSM-predicted responses, including the optimum (fit) and confirmatory replicate (uncoded units).
| Entry | X1 (temp, °C) | X2 (time, min) | X3 (amp, %) | TPC exp (mg GAE/100 ml) | TPC Pred | FRAP exp (mmol TE/L) | FRAP pred |
|---|---|---|---|---|---|---|---|
| 1 | 45 | 6.00 | 70.00 | 143.91 | 143.50 | 12.04 | 11.92 |
| 2 | 50 | 8.00 | 80.00 | 137.30 | 139.97 | 10.56 | 10.86 |
| 3 | 45 | 6.00 | 90.00 | 107.84 | 108.97 | 10.65 | 10.56 |
| 4 | 45 | 10.00 | 90.00 | 105.95 | 106.15 | 9.89 | 9.79 |
| 5 | 50 | 12.00 | 80.00 | 95.94 | 95.28 | 8.43 | 8.32 |
| 6 | 50 | 8.00 | 60.00 | 113.34 | 113.21 | 10.23 | 10.12 |
| 7 | 55 | 6.00 | 70.00 | 126.71 | 127.88 | 11.57 | 11.69 |
| 8 | 55 | 10.00 | 70.00 | 101.14 | 101.38 | 9.24 | 9.33 |
| 9 | 55 | 6.00 | 90.00 | 139.21 | 138.97 | 11.70 | 11.59 |
| 10 | 50 | 8.00 | 80.00 | 140.38 | 139.97 | 10.95 | 10.86 |
| 11 | 50 | 8.00 | 80.00 | 139.94 | 139.97 | 10.95 | 10.86 |
| 12 | 55 | 10.00 | 90.00 | 118.17 | 119.97 | 9.45 | 9.58 |
| 13 | 50 | 4.00 | 80.00 | 124.10 | 124.59 | 11.34 | 11.45 |
| 14 | 50 | 8.00 | 80.00 | 141.71 | 139.97 | 11.06 | 10.86 |
| 15 | 50 | 8.00 | 100.00 | 97.31 | 97.27 | 8.90 | 9.00 |
| 16 | 40 | 8.00 | 80.00 | 135.83 | 135.76 | 12.44 | 12.54 |
| 17 | 60 | 8.00 | 80.00 | 134.06 | 133.96 | 12.22 | 12.10 |
| 18 | 50 | 8.00 | 80.00 | 137.74 | 139.97 | 10.77 | 10.86 |
| 19 | 50 | 8.00 | 80.00 | 141.71 | 139.97 | 10.90 | 10.86 |
| 20 | 45 | 10.00 | 70.00 | 131.56 | 133.18 | 10.67 | 10.80 |
| OPT (fit) | 40 | 6.75 | 64.04 | 154.63 | 13.25 | ||
| OPT (exp rep.) | 40 | 6.75 | 64.04 | 149.77 | 12.86 |
X1, temperature (°C); X2, processing time (min); X3, ultrasound amplitude (%); FRAP, ferric reducing antioxidant power; TPC, total phenolic content; TE, Trolox equivalents; GAE, gallic acid equivalents; Exp, experimental; Pred, predicted; RSM, response surface methodology.