Table 2.
[NH4Ac] (M) | 9+ | 8+ | 7+ | 6+ |
---|---|---|---|---|
0 | 36 ± 8 | 29 ± 3 | 53 ± 8 | <DL |
1.0 × 10−3 | 25 ± 2 | 29 ± 6 | 72 ± 10 | <DL |
1.0 × 10−1 | <DL | 48 ± 15 | 76 ± 10 | 82 ± 5 |
8 | <DL | 20 ± 2 | 23 ± 5 | 26 ± 4 |
For 0, 1.0 × 10−3, and 1.0 × 10−1 M NH4Ac, the adducts are due to sodium (+22 Da; Na+ displaces H+). For 8 M NH4Ac, the adducts are due to ammonia (17 Da) and acetic acid (60 Da). Reported errors are ±1 standard deviation from the mean for three replicate measurements. <DL indicates that a given charge state is below detection limits.