| Crystal data |
| Chemical formula |
C27H28O5
|
|
M
r
|
432.49 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
258 |
|
a, b, c (Å) |
5.435 (2), 14.445 (5), 15.277 (5) |
| α, β, γ (°) |
95.104 (11), 95.693 (12), 99.725 (12) |
|
V (Å3) |
1169.3 (7) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.08 |
| Crystal size (mm) |
0.38 × 0.32 × 0.27 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.965, 0.975 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
30609, 6801, 4287 |
|
R
int
|
0.041 |
| (sin θ/λ)max (Å−1) |
0.705 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.062, 0.155, 1.03 |
| No. of reflections |
6801 |
| No. of parameters |
289 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.17, −0.19 |
