Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C22H17ClN2O2S2 |
| M r | 440.94 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 300 |
| a, b, c (Å) | 20.7798 (3), 13.1963 (4), 16.1047 (4) |
| β (°) | 102.440 (3) |
| V (Å3) | 4312.49 (19) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.39 |
| Crystal size (mm) | 0.35 × 0.25 × 0.18 |
| Data collection | |
| Diffractometer | Bruker D8 Venture Diffractometer |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 53818, 3823, 2660 |
| R int | 0.117 |
| (sin θ/λ)max (Å−1) | 0.597 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.051, 0.133, 1.06 |
| No. of reflections | 3823 |
| No. of parameters | 263 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.21, −0.34 |