Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C24H14F2N2O2 |
| M r | 400.37 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 13.767 (8), 16.914 (11), 8.447 (5) |
| β (°) | 104.423 (13) |
| V (Å3) | 1904.9 (19) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.10 |
| Crystal size (mm) | 0.3 × 0.2 × 0.1 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.617, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 10872, 3740, 1446 |
| R int | 0.110 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.076, 0.151, 0.91 |
| No. of reflections | 3740 |
| No. of parameters | 272 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.20, −0.19 |