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. 2026 Sep 11;82(Pt 10):1179–1183. doi: 10.1107/S2056989026009394

Table 3. Experimental details.

Crystal data
Chemical formula C24H14F2N2O2
M r 400.37
Crystal system, space group Monoclinic, P21/c
Temperature (K) 296
a, b, c (Å) 13.767 (8), 16.914 (11), 8.447 (5)
β (°) 104.423 (13)
V (Å3) 1904.9 (19)
Z 4
Radiation type Mo Kα
μ (mm−1) 0.10
Crystal size (mm) 0.3 × 0.2 × 0.1
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Krause et al., 2015 ▸)
Tmin, Tmax 0.617, 0.746
No. of measured, independent and observed [I > 2σ(I)] reflections 10872, 3740, 1446
R int 0.110
(sin θ/λ)max (Å−1) 0.617
 
Refinement
R[F2 > 2σ(F2)], wR(F2), S 0.076, 0.151, 0.91
No. of reflections 3740
No. of parameters 272
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.20, −0.19

Computer programs: APEX2 and SAINT (Bruker, 2008 ▸), SHELXT2018/2 (Sheldrick, 2015a ▸), SHELXL2019/3 (Sheldrick, 2015b ▸) and OLEX2 (Dolomanov et al., 2009 ▸).