Table 2. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| O4—H4⋯O7 | 0.82 | 1.75 | 2.562 (4) | 174 |
| O2—H2⋯O3 | 0.82 | 1.84 | 2.647 (3) | 169 |
| O7—H7A⋯O1 | 0.85 | 1.88 | 2.709 (4) | 163 |
| O7—H7B⋯S2i | 0.85 | 2.64 | 3.290 (3) | 135 |
| O5—H5A⋯O6 | 0.82 | 1.94 | 2.655 (6) | 146 |
| C18—H18A⋯Br3ii | 0.97 | 3.32 | 3.856 (4) | 117 |
| C18—H18A⋯S1 | 0.97 | 2.98 | 3.801 (4) | 143 |
| C18—H18A⋯N3 | 0.97 | 3.22 | 3.785 (5) | 119 |
| C17—H17A⋯O5 | 0.97 | 2.73 | 3.368 (5) | 124 |
| C16—H16⋯O6iii | 0.93 | 2.52 | 3.376 (5) | 153 |
| C2—H2A⋯O2iv | 0.93 | 2.92 | 3.726 (4) | 146 |
| C2—H2A⋯O7 | 0.93 | 3.08 | 3.548 (5) | 113 |
| C9—H9A⋯N4v | 0.97 | 3.20 | 3.851 (4) | 126 |
| C9—H9B⋯O3v | 0.97 | 3.03 | 3.613 (5) | 120 |
| C9—H9B⋯N4 | 0.97 | 3.20 | 3.700 (5) | 114 |
| C11—H11⋯S2v | 0.93 | 3.11 | 3.709 (4) | 124 |
| C8—H8A⋯S1vi | 0.97 | 3.29 | 3.881 (3) | 121 |
| C8—H8A⋯O3v | 0.97 | 3.07 | 3.773 (5) | 130 |
| C8—H8B⋯S2iii | 0.97 | 3.30 | 3.784 (4) | 113 |
| C8—H8B⋯O7vi | 0.97 | 2.96 | 3.739 (6) | 138 |
| C14—H14⋯O6iii | 0.93 | 3.12 | 3.827 (6) | 134 |
| C12—H12⋯S2v | 0.93 | 2.93 | 3.616 (5) | 131 |
| C22—H22⋯O6iii | 0.93 | 2.97 | 3.847 (6) | 158 |
| C27—H27⋯Br2vii | 0.93 | 3.04 | 3.949 (6) | 166 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.