| Crystal data |
| Chemical formula |
[U(C5H7O2)2O2(C5H4Cl2N2)]·0.5CH4O |
|
M
r
|
647.26 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
273 |
|
a, b, c (Å) |
8.1200 (13), 11.7640 (19), 22.830 (4) |
| α, β, γ (°) |
97.657 (3), 91.181 (3), 97.175 (3) |
|
V (Å3) |
2142.9 (6) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
7.86 |
| Crystal size (mm) |
0.30 × 0.05 × 0.05 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.453, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
11317, 7468, 4722 |
|
R
int
|
0.052 |
| (sin θ/λ)max (Å−1) |
0.596 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.057, 0.178, 1.01 |
| No. of reflections |
7468 |
| No. of parameters |
494 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.29, −1.59 |
