| Crystal data |
| Chemical formula |
[Zn(C2H3O2)2(C7H5FN2S)2] |
|
M
r
|
519.88 |
| Crystal system, space group |
Orthorhombic, Pna21
|
| Temperature (K) |
273 |
|
a, b, c (Å) |
8.26379 (13), 27.6342 (3), 9.21400 (12) |
|
V (Å3) |
2104.14 (5) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
3.95 |
| Crystal size (mm) |
0.37 × 0.28 × 0.25 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Single source at home/near, HyPix3000 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2023 ▸) |
|
Tmin, Tmax
|
0.336, 1.000 |
| No. of measured, independent and observed [I ≥ 2σ(I)] reflections |
19982, 4036, 3829 |
|
R
int
|
0.063 |
| (sin θ/λ)max (Å−1) |
0.616 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.040, 0.113, 1.03 |
| No. of reflections |
4036 |
| No. of parameters |
282 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.38, −0.60 |
| Absolute structure |
Hooft et al. (2010 ▸) |
| Absolute structure parameter |
0.002 (12) |
