| Crystal data |
| Chemical formula |
C15H12FNO4
|
|
M
r
|
289.26 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
8.4674 (9), 9.2193 (11), 9.2749 (11) |
| α, β, γ (°) |
102.838 (4), 96.181 (4), 108.027 (4) |
|
V (Å3) |
659.01 (13) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.12 |
| Crystal size (mm) |
0.35 × 0.30 × 0.21 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.954, 0.966 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
8198, 2722, 2050 |
|
R
int
|
0.036 |
| (sin θ/λ)max (Å−1) |
0.627 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.039, 0.102, 1.05 |
| No. of reflections |
2722 |
| No. of parameters |
236 |
| No. of restraints |
12 |
| H-atom treatment |
Only H-atom coordinates refined |
| Δρmax, Δρmin (e Å−3) |
0.24, −0.26 |
