Table 3. Hydrogen-bond geometry (Å, °) for 2.
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| C7—H7⋯O10i | 0.95 | 2.60 | 3.5233 (16) | 165 |
| C36—H36⋯O14ii | 0.95 | 2.45 | 3.3930 (17) | 172 |
| C44—H44B⋯O11iii | 0.98 | 2.58 | 3.4643 (19) | 151 |
| O10—H10A⋯O1 | 0.87 | 2.21 | 2.9342 (15) | 140 |
| O10—H10A⋯O2 | 0.87 | 2.28 | 3.0393 (14) | 146 |
| O10—H10B⋯O3 | 0.87 | 2.42 | 3.1432 (14) | 141 |
| O10—H10B⋯O4 | 0.87 | 2.28 | 3.0579 (15) | 148 |
| O11—H11A⋯O3 | 0.87 | 2.11 | 2.9635 (15) | 169 |
| O11—H11B⋯O1 | 0.87 | 2.48 | 3.2974 (16) | 157 |
| O11—H11B⋯O2 | 0.87 | 2.52 | 3.0582 (15) | 121 |
| O12—H12A⋯O10 | 0.87 | 2.00 | 2.8520 (19) | 167 |
| O12—H12B⋯O11 | 0.87 | 2.23 | 2.9457 (19) | 139 |
| O13—H13A⋯O5 | 0.87 | 2.11 | 2.8255 (14) | 139 |
| O13—H13A⋯O6 | 0.87 | 2.27 | 3.0237 (13) | 145 |
| O13—H13B⋯O7 | 0.87 | 2.30 | 3.0580 (14) | 146 |
| O13—H13B⋯O8 | 0.87 | 2.08 | 2.8108 (14) | 141 |
| O14—H14A⋯O12iv | 0.87 | 1.99 | 2.8457 (17) | 167 |
| O14—H14B⋯O13 | 0.87 | 2.01 | 2.8683 (18) | 167 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
.