Table II. Heavy atom derivative statistics for rClfA(221–559).
Heavy atom compound | Resolution (Å) | Rsyma (%) | Unique reflections | Solve |
Phases |
||
---|---|---|---|---|---|---|---|
Rcentric | R.M.S. (FH)/R.M.S.(E) | Rcullisb | Phasing powerc | ||||
(CH3)3PbOOCCH3 | 2.45 | 6.2 | 13 162 | 0.57 | 1.35 | 0.567 | 1.98 |
K2PtCl4 | 3.2 | 16.3 | 7177 | 0.64 | 1.22 | 0.657 | 1.15 |
PCMBS | 3.0 | 7.2 | 7450 | 0.56 | 1.42 | 0.628 | 1.45 |
aRsym = Σ|Ih – <Ih>|/ΣIh, where <Ih> is the average intensity over symmetry equivalents.
bRcullis = Σ||FPH ± FP| – FHcalc|/Σ|FPH – FP|
cPhasing power = Σ|FH|/Σ||FPHobs| – |FPHcalc||