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. 2006 Mar 3;2:3. doi: 10.1186/1860-5397-2-3

Table 3.

The penalty points for example 2

# 1–6 from Table 1 Penalty

1 Yield: 87% 6
2 H2O2 (30%, 4.1 mL, 36 mmol) 0
Na2WO4·2H2O (66 mg, 0.2 mmol) 0
[(Octyl)3NMe]HSO4 (93 mg, 0.2 mmol) 0
Molecular sieves 4Å (100 mg) 0
3 Benzyl chloride (T) 5
4 Dropwise addition of H2O2 1
5 90°C, 10 h 3
6 Extraction with AcOEt (3 × 10 mL) 3
Washing with aq. Na2S2O4 3
Drying over MgSO4 0
Removal of AcOEt 0
Crystallization from hexanes 1

Penalty points total: 22