Table 1.
Data processing, refinement, and model (2GD4)
| Crystal | ||
| Space group | C2 | |
| Cell dimensions (Å) | a=220.26, b=60.59, c=156.17, β=113.14 | |
| Solvent content (%) | 51.6 | |
| Data-processing statistics | ||
| Wavelength (Å) | 1.488 (SRS Daresbury, station 14.1) | |
| Resolution (Å) | 36.91–3.30 | 3.48–3.30 |
| Total reflections | 50 549 | 7380 |
| Unique reflections | 27 231 | 3981 |
| Multiplicity | 1.9 | 1.9 |
| 〈I〉/σ(〈I〉) | 5.8 | 1.9 |
| Completeness (%) | 94.6 | 95.1 |
| Rmerge | 0.175 | 0.476 |
| Model | ||
| Number of atoms modeled: | ||
| Protein | 10 763 | |
| Water | 63 | |
| Carbohydrate | 155 | |
| Ligand (fondaparinux) | 182 | |
| Calcium ions | 2 | |
| Average B-factor (Å2) | 38.9 | |
| Refinement statistics | ||
| Resolution range (Å) | 35.23–3.30 | 3.51–3.30 |
| Reflections in working/free set | 26 110/1114 | 4349/186 |
| R-factor/R-free (%) | 24.7/29.7 | 31.2/35.1 |
| RMSD of bonds (Å)/angles (deg) from ideality | 0.009/1.5 | |
| Ramachandran plot; residues in | ||
| Most favored region (%) | 68.2 | |
| Additionally allowed region (%) | 28.2 | |
| Generously allowed region (%) | 3.3 | |
| Disallowed region (%) | 0.3 | |