Table 1. Summary of data collection and refinement statistics.
| Data collection | invE190–raffinose complex |
|---|---|
| X-ray source | ESRF (ID14-EH2) |
| Wavelength (Å) | 0.934 |
| Resolution range (Å) | 32.1–1.87 (1.94–1.87) |
| Space group | P 21 |
| Rsym | 0.040 (0.18) |
| Completeness (%) | 97.7 (91.7) |
| I/σI | 16.2 (5.5) |
| Number of unique reflections | 220454 (20270) |
| Refinement statistics | |
| Resolution range (Å) | 32.1–1.87 (1.94–1.87) |
| Rcryst (%) | 19.8 (21.7) |
| Rfree (%) | 22.9 (26.1) |
| Overall B-factor (Å2) | 25.5 |
| R.M.S.D. in bond lengths (Å) | 0.006 |
| R.M.S.D. in bond angles (°) | 1.103 |
| Ramachandran plot | |
| Most favoured regions (%) | 88.3 |
| Additionally allowed regions (%) | 10.7 |