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. Author manuscript; available in PMC: 2006 Jun 14.
Published in final edited form as: Angew Chem Int Ed Engl. 2004 Sep 13;43(36):4788–4791. doi: 10.1002/anie.200460612

Scheme 3.

Scheme 3

Preparation of the enantiomerically enriched allylic carbonate electrophile. BOC-ON=2-(tert-butoxycarbonyloxyimino)-2-phenylacetonitrile, DCHT=dicyclohexyl tartrate, MS=molecular sieves, TBHP=tert-butyl hydroperoxide, TBS=tert-butyldimethylsilyl.