Table 1. Crystallographic parameters and refinement statistics.
Parameter | Value |
---|---|
X-ray source | Synchroton radiation |
Wavelength (Å) | 1.03 |
Cell Parameters | a = b = 37.81 Å; c = 63.02 Å |
α = β = γ = 90° | |
Space group | P43212 |
No. of unique reflections | 2621 |
Completeness (%) | 95.4 (75.6) |
No. of reflections [> 2σ (Fo)] | 2321 |
<I/σ(I)>a | 5.4 (1.37) |
Resolution range (Å) | 8–2.15 |
R-merge (%)b | 11.8 (53.1) |
R-factor (%) | 22.4 |
R-free (%)c | 23.3 |
Rmsd of bonds from ideality (Å) | 0.013 |
aValues in parenthesis relate to the highest resolution shell (2.17–2.15 Å).
bR-merge = Σ |I – <I>| /Σ<I>.
cCalculated using 10% of data.