Table 1.
Crystallographic data and refinement statistics
| Native data | Single anomalous dispersion data | |
|---|---|---|
| Data collection statistics | ||
| Wavelength, Å | 1.07216 | 1.06287 |
| Space group | I23 | I23 |
| Cell dimensions, Å | a = b = c = 100.1 | a = b = c = 100.4 |
| Mosaicity, ° | 0.2 | 0.3 |
| Oscillation range, ° | 1.0 | 1.0 |
| PtCl4 sites | — | 2 |
| Resolution, Å | 20–1.7 (1.76–1.70)* | 20–1.8 (1.86–1.80) |
| Total/unique reflections | 195,458/18,534 | 190,992/30,303 |
| Completeness, % | 100 (100) | 100 (100) |
| Rsym, % | 7.9 (16.9) | 7.4 (33) |
| Refinement statistics | ||
| Resolution, Å | 20–1.7 | |
| No. of water atoms | 102 | |
| No. of protein atoms | 1026 | |
| No. of heteroatoms (PO4, GlcNAc) | 19 | |
| Rwork/Rfree, % | 19.5/21.3 | |
| rms deviation bond lengths, Å | 0.01 | |
| rms deviation bond angles, ° | 1.6 | |
| Average B factor, Å2 | 12.3 |
*
Values in parentheses are for the reflections in the highest resolution shell.