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The x-ray diffractograms of nanocrystalline ZrO2⋅Y2O3 specimens allow the determination of the crystallite size d from the line broadening and a qualitative analysis of the crystal structure. Depending on the dopant concentration, tetragonal (a) and cubic (b) specimens, which can be distinguished by the C{400} reflection, were obtained after sintering at TA. The cubic specimens were used for the diffusion experiments.
