Table 1.
1H chemical shifts in P2 peptide
| Residue | δ(HN)/3JHNα | δ(Hα) | δ(Hβ) | Others |
|---|---|---|---|---|
| Asp-1 | 8.71/6.0 | 4.48 | 2.63, 2.37 | N-term CH3 1.92 |
| Lys-2 | 8.39/7.5 | 4.41 | 1.98, 1.86 | Hγ 1.58; Hδ 1.68; Hɛ 3.01; Hζ 7.48 |
| Asp-3 | 8.07/9.1 | 4.75 | 3.13, 2.61 | |
| Gly-4 | 7.99 | 3.89, 3.79 | ||
| Asp-5 | 7.81/8.8 | 4.70 | 3.22, 2.67 | |
| Gly-6 | 9.04 | 4.00, 3.52 | ||
| Tyr-7 | 8.50/8.4 | 4.88 | 2.95, 2.70 | Hδ 7.03; Hɛ 6.80 |
| Ile-8 | 9.53/9.7 | 4.47 | 1.83 | γCH2 1.57; γCH3 0.86; Hδ 0.86 |
| Ser-9 | 9.78/6.9 | 4.51 | 4.44, 4.10 | |
| Ala-10 | 9.09/3.0 | 4.19 | 1.49 | |
| Ala-11 | 8.53/4.6 | 4.20 | 1.42 | |
| Glu-12 | 8.04/5.8 | 4.02 | 2.40, 2.13 | Hγ 2.57, 2.31 |
| Ala-13 | 8.79/4.4 | 4.11 | 1.45 | |
| Ala-14 | 7.89/5.1 | 4.20 | 1.49 | |
| Ala-15 | 7.58/5.8 | 4.28 | 1.49 | |
| Gln-16 | 7.75/7.1 | 4.21 | 2.19, 2.13 | Hγ 2.50, 2.42; Hɛ 7.36, 7.33 |
| NH2 | 7.66, 6.90 |