Table 1. Data collection statistics for OpdA at 7132, 7725 and 9576 eV.
Value | ||||
---|---|---|---|---|
Parameter | Edge… | Fe–K (7132 eV) | Co–K (7725 eV) | Zn–K (9576 eV) |
Space group | P3121 | P3121 | P3121 | |
a=108.9, c=62.4 Å | a=108.9, c=62.4 Å | a=108.9, c=62.4 Å | ||
Number of observations | 351555 | 360482 | 368460 | |
Number of unique reflections | 33940 | 33957 | 33964 | |
Completeness (%) | 100 | 100 | 100 | |
〈I/σ(I)〉 | 29.9 | 30.7 | 31.0 | |
Resolution range (Å) | ||||
Overall | 62.0–1.9 | 62.0–1.9 | 62.0–1.9 | |
Outer | 2.0–1.9 | 2.0–1.9 | 2.0–1.9 | |
Rscal (overall/outer shell) | 6.3/23.0 | 6.2/22.9 | 6.1/20.7 |