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. 2006 Jul 20;25(15):3675–3683. doi: 10.1038/sj.emboj.7601240

Table 1.

Summary of data collection and refinement statistics

Data set Native Se-Met
Data collection statistics
Space group R32 R32
Cell dimensions
a, c (Å) 129.93, 122.49 131.05, 122.57
Wavelength (Å) 0.90000 0.97887
Resolution (Å) 50.0–2.05 (2.12–2.05) 54.0–2.32 (2.44–2.32)
No. of reflections
 Observed 174 011 157 273
 Unique 24 374 (2255) 17 032 (1890)
Completeness (%) 96.8 (91.1) 96.2 (74.1)
Redundancy 6.9 (6.8) 9.2 (6.2)
Rmerge 7.2 (41.5) 8.4 (54.5)
I/σ(I)〉 13.7 (4.7) 5.1 (1.3)
     
Refinement statistics    
Resolution (Å) 50.0–2.05  
No. of reflections used  
 Working set/test set 22 548/1254  
Rwork/Rfree (%) 23.4/26.5  
No. of atoms  
 Protein 2362  
 Ion 3  
 Water 100  
B-factors
 Protein 51.3  
  Sub-A 74.2  
  EGF 63.0  
  Sub-B 33.1  
 Ion 39.0  
 Water 41.6  
R.m.s.d. from ideality  
 Bond lengths (Å) 0.010  
 Bond angles (deg) 1.269