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Experimental Values To Determine Theoretical Band Broadening Contributions from the Flow Reactor
| trial 1
|
trial 2
|
|||
|---|---|---|---|---|
| YGGFM | YGGFL | YGGFM | YGGFL | |
| fwhm (s) | 8.1 (4)a | 11.1 (4) | 8.0 (6) | 10.8 (6) |
| σt column (s) | 3.4 (4) | 4.7 (4) | 3.4 (4) | 4.6 (4) |
| D (cm2/s) | 4.1 × 10−6 | 4.1 × 10−6 | ||
| σt2/t | 0.064 | 0.064 | ||
| residence time (s) | 12.0 | 11.2 | ||
| σt reactor (s) | 0.88 | 0.85 | ||
| % broadening from reactor | 3.2 | 1.7 | 3.0 | 1.7 |
Number of chromatogram.
