Table 1.
Unit-cell parameters | ||
---|---|---|
a (Å) | 145 | |
b (Å) | 145 | |
c (Å) | 498 | |
α (°) | 90 | |
β (°) | 90 | |
γ (°) | 90 | |
Temperature (K) | 100 | |
Space group | P41212 | |
Molecules in asymmetric unit | 1 | |
Solvent content (%) | ∼73 | |
Resolution (Å) | 2.5 (2.59–52.5) | |
Observations | 749 175 | |
Unique reflections | 193 488 | |
Rmergea | 0.102 (0.432) | |
Completeness (%) | 91.3 (83.5) | |
I/σ(I) | 14.4 (2.8) |
Values in parentheses are for highest resolution shell.
aRmerge = , where Ij is the intensity of reflection j and (Ij) is the average intensity of reflection j.