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NMR parameters of 1-glyceryl-1-myo-inosityl-phosphate
| Moiety | 13C NMR δ (ppm) |
1H NMR
|
31P NMR
|
||
|---|---|---|---|---|---|
| δ (ppm) | nJH,H (Hz) | δ (ppm) | nJP,X (Hz) | ||
| Inositol | |||||
| C1 | 77.0 | 3.97 | 3J1,2 = 2.75 | 2JP,C = 6.24 | |
| C2 | 71.9 | 4.27 | 3J2,3 = 2.75 | ||
| C3 | 71.4 | 3.56 | 3J3,4 = 9.92 | ||
| C4 | 72.9 | 3.66 | 3J4,5 = 9.60 | ||
| C5 | 74.6 | 3.34 | 3J5,6 = 9.31 | ||
| C6 | 72.1 | 3.76 | 3J6,1 = 10.0 | ||
| Glycerol | |||||
| C1 | 67.1 | 3.98/3.94 | NDa | 2JP,C = 5.76 | |
| C2 | 71.5 | 3.92 | 3J2,3a = 4.13 3J2,3b = 6.20 | 3JP,C = 6.72 | |
| C3 | 62.8 | 3.69/3.61 | 2J3a,3b = 12.40 | ||
| Phosphate | 0.4 | ||||
ND, not determined.
