TABLE 1.
Resolution range (Å) | No. of unique reflections | Phase residual (°)b |
---|---|---|
∞-22.4 | 23 | 22.2 |
22.4-15.8 | 24 | 25.0 |
15.8-12.8 | 20 | 15.5 |
12.8-11.1 | 21 | 7.3 |
11.1-9.9 | 25 | 13.8 |
9.9-9.1 | 18 | 32.1 |
9.1-8.4 | 25 | 24.1 |
8.4-7.8 | 26 | 19.2 |
7.8-7.4 | 22 | 16.3 |
7.4-7.0 | 19 | 27.3 |
∞-7.0 | 223 | 21.0 |
Number of images, 6; plane group, p1; cell parameters, 99.2 ± 0.9 Å (a), 98.5± 0.4 Å (b), and 131.1 ± 0.3° (β); defocus range, 3,530 to 5,450 Å.
The random phase residual was 90°.