Table 1.
Data collection and refinement statistics for the yeast F1 ATPase
| Data collection | |
|---|---|
| Space group | P21 |
| Cell parameters (Å and deg) | a=111.5, b=294.1, c=190.4, β=101.7 |
| Resolution (Å) | 2.8 |
| Number of reflections | 293 909 |
| Rmergea,b | 8.7 (37.6) |
| 〈I/σ(I)〉b | 13.9 (3.0) |
| Completenessb | 99.9 (99.7) |
| Mean multiplicityb | 5.1 (3.9) |
| Refinement statistics | |
| R-factorb (%) | 20.7 |
| Rfreeb,c (%) | 24.4 |
| R.m.s. deviations from standard values | |
| Bonds (Å) | 0.011 |
| Angles (deg) | 1.3 |
| aRmerge=∑∑i∣Ihi–〈Ih〉∣/∑∑Ihi, where 〈Ih〉 is the weighted mean intensity for all observations of reflections h after rejection of outliers. | |
| bThe statistics for the highest resolution shell (2.95–2.80 Å) are given in brackets. | |
| cRfree was calculated for 5942 reflections, which were excluded from the refinement. | |